Volume : IV, Issue : IX, September - 2015
SYNTHESIS OF N – HYDROXY – 3, 3 – DIMETHYL – 2, 6 – DIARYL PIPERIDIN – 4 – ONE THIOSEMI CARBAZONE
Dr. S. Tamilselvi, Dr. K. G. Palani
Abstract :
N – hydroxyl – 3, 3 – dimethyl – 2, 6 – diaryl piperidin – 4 – one thiosemicarbazone is synthesized by the reaction of N – hydroxyl – 3, 3 – dimethyl – 2, 6 – diaryl piperidin – 4 – one oxime & thiosemicarbazied in presence of (Si O2 & DCC) silicandioxide & dicyclo hcxyl carbodimide heterogeneous catalyst under microwave irradiation. The structure of the thiosemicarbazone is confirmed by elemental analysis, 1H NMR and 13C NMR spectral studies.
Keywords :
N � hydroxyl � 3 3 � dimethyl � 2 6 � diaryl piperidin � 4 � one thiosemicarbazone 1H and 13C NMR.
Article:
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DOI : https://www.doi.org/10.36106/gjra
Cite This Article:
Dr. S. TAMILSELVI, Dr. K.G. PALANI Synthesis of N � Hydroxy � 3, 3 � Dimethyl � 2, 6 � Diaryl Piperidin � 4 � One Thiosemi Carbazone Global Journal For Research Analysis, Vol: 4, Issue: 9 September 2015
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Dr. S. TAMILSELVI, Dr. K.G. PALANI Synthesis of N � Hydroxy � 3, 3 � Dimethyl � 2, 6 � Diaryl Piperidin � 4 � One Thiosemi Carbazone Global Journal For Research Analysis, Vol: 4, Issue: 9 September 2015