Volume : VI, Issue : VII, July - 2017

GROWTH OF ROD-SHAPED Sb2S3 NANO COMPOUNDS UNDER MILD REACTION CONDITION

Nilkamal Maiti

Abstract :

 One-dimensional (1D) rod-shaped nano compounds of Sb₂S₃ have been achieved from SbCl₃ and S-methyl 3-phenyldithiocarbazate [C₆H₅NHNHC(S)SMe] via a simple and mild solvothermal method in ethanol without any surfactants or additives. The products have been characterized by X-ray powder diffraction (XRD) and transmission electron microscopy (TEM). From this experiment it showed that the rod-shaped Sb₂S₃ nanocrystals, belong to the orthorhombic phase with cell parameters a = 11.305 Å, b = 11.277 Å, c = 3.952 Å. The probable formation mechanism of rod shaped nano structure of Sb₂S₃ has also been proposed.

 

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Article: Download PDF    DOI : https://www.doi.org/10.36106/gjra  

Cite This Article:

Nilkamal Maiti, GROWTH OF ROD-SHAPED Sb2S3 NANO COMPOUNDS UNDER MILD REACTION CONDITION, GLOBAL JOURNAL FOR RESEARCH ANALYSIS : VOLUME-6 | ISSUE‾7 | JULY -2017

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